Optically detected magnetic resonance of nitrogen vacancies in a diamond anvil cell using designer diamond anvils

Optically detected magnetic resonance of nitrogen vacancy centers in diamond offers a route to both DC and AC magnetometry in diamond anvil cells under high pressures (>3 GPa). However, a serious challenge to realizing experiments has been the insertion of microwave radiation into the sample space without screening by the gasket material. We utilize designer anvils with lithographically deposited metallic microchannels on the diamond culet as a microwave antenna. We detected the spin resonance of an ensemble of microdiamonds under pressure and measured the pressure dependence of the zero field splitting parameters. These experiments enable the possibility for all-optical magnetic resonance experiments on nanoliter sample volumes at high pressures.

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7 pages, 4 figures

References(30)

Figures(7)

[1]

Pressure-induced superconductivity in quasi-2D CeRhIn5

H. Hegger
,
C. Petrovic
,
E.G. Moshopoulou
,
M.F. Hundley
,
J.L. Sarrao

et al.

- Phys.Rev.Lett. 84 (2000) 4986-4989
•
DOI:
- 10.1103/PhysRevLett.84.4986

[2]

Superconductivity up to 29 K in SrFe2As2 and BaFe2As2 at high pressures

P.L. Alireza
,
Y.T.C. Ko
,
J. Gillett
,
C.M. Petrone
,
J.M. Cole

et al.

- J.Phys.Condens.Matter 21 (2009) 012208
•
DOI:
- 10.1088/0953-8984/21/1/012208

[3]

Observation of the Wigner-Huntington transition to metallic hydrogen

R.P. Dias
,
I.F. Silvera

- Science 355 (2017) 715-718
•
DOI:
- 10.1126/science.aal1579

[4]

Spontaneous formation of a superconducting and antiferromagnetic hybrid state in SrFe2As2 under high pressure

K. Kitagawa
,
N. Katayama
,
H. Gotou
,
T. Yagi
,
K. Ohgushi

et al.

- Phys.Rev.Lett. 103 (2009) 257002
•
DOI:
- 10.1103/PhysRevLett.103.257002

[5]

Evolution of hyperfine parameters across a quantum critical point in CeRhIn5

C.H. Lin
,
K.R. Shirer
,
J. Crocker
,
A.P. Dioguardi
,
M.M. Lawson

et al.

- Phys.Rev.B 92 (2015) 155147
•
DOI:
- 10.1103/PhysRevB.92.155147

[6]

10 GPa-class high-pressure NMR technique realized by the new cell with improved space efficiency

K. Kitagawa
,
K. Matsubayashi
,
H. Gotou
,
T. Matsumoto
,
Y. Uwatoko

et al.

- Sci.Technol. 22 (2012) 198-205
•
DOI:
- 10.4131/jshpreview.22.198

[7]

High-sensitivity NMR beyond 200,000 atmospheres of pressure

T. Meier
,
S. Reichardt
,
J. Haase

- J.Magn.Resonance 257 (2015) 39-44
•
DOI:
- 10.1016/j.jmr.2015.05.007

[8]

NMR in a diamond anvil cell

S.-H. Lee
,
K. Luszczynski
,
R.E. Norberg
,
M.S. Conradi

- Rev.Sci.Instrum. 58 (1987) 415-417
•
DOI:
- 10.1063/1.1139246

[9]

Molecular motion in solid H2 at high pressures

S.-H. Lee
,
M.S. Conradi
,
R.E. Norberg

- Phys.Rev.B 40 (1989) 12492-12498
•
DOI:
- 10.1103/PhysRevB.40.12492

[10]

Nuclear magnetic resonance in a diamond anvil cell at very high pressures

M.G. Pravica
,
I.F. Silvera

- Rev.Sci.Instrum. 69 (1998) 479
•
DOI:
- 10.1063/1.1148686

[11]

Electronic Properties and Metrology Applications of the Diamond ${NV}^{-}$ Center under Pressure

et al.

- Phys.Rev.Lett. 112 (2014) 4, 047601
•
DOI:
- 10.1103/PhysRevLett.112.047601

[12]

Properties of nitrogen-vacancy centers in diamond: the group theoretic approach

et al.

- New J.Phys. 13 (2011) 2, 025025
•
DOI:
- 10.1088/1367-2630/13/2/025025

[13]

Ultralong spin coherence time in isotopically engineered diamond

et al.

- Nature Materials 8 (2009) 5, 383-387
•
DOI:
- 10.1038/nmat2420

[14]

Solid-state electronic spin coherence time approaching one second

- Nature Commun. 4 (2013) 1, 1743
•
DOI:
- 10.1038/ncomms2771

[15]

Realtime magnetic field sensing and imaging using a single spin in diamond

- Phys.Rev.Lett. 106 (2011) 030802
•
e-Print:
- 1009.4138
•
DOI:
- 10.1103/PhysRevLett.106.030802

[16]

Room Temperature Operation of a Radiofrequency Diamond Magnetometer near the Shot Noise Limit

et al.

- J.Appl.Phys. 112 (2012) 124519
•
e-Print:
- 1201.3152
•
DOI:
- 10.1063/1.4771924

[17]

Atomic-scale nuclear spin imaging using quantum-assisted sensors in diamond

A. Ajoy
,
U. Bissbort
,
M.D. Lukin
,
R.L. Walsworth
,
P. Cappellaro

- Phys.Rev.X 5 (2015) 011001
•
DOI:
- 10.1103/PhysRevX.5.011001

[18]

Nuclear Magnetic Resonance Spectroscopy on a (5-Nanometer)3 Sample Volume

et al.

- Science 339 (2013) 6119, 1231675
•
DOI:
- 10.1126/science.1231675

[19]

Nanoscale Nuclear Magnetic Resonance with a Nitrogen-Vacancy Spin Sensor

et al.

- Science 339 (2013) 6119, 1231540
•
DOI:
- 10.1126/science.1231540

[20]

An electrical microheater technique for high-pressure and high-temperature diamond anvil cell experiments

S.T. Weir
,
D.D. Jackson
,
S. Falabella
,
G. Samudrala
,
Y.K. Vohra

- Rev.Sci.Instrum. 80 (2009) 013905-013910
•
DOI:
- 10.1063/1.3069286

[21]

Magnetic susceptibility measurements at high pressure using designer diamond anvils

D.D. Jackson
,
C. Aracne-Ruddle
,
V. Malba
,
S.T. Weir
,
S.A. Catledge

et al.

- Rev.Sci.Instrum. 74 (2003) 2467
•
DOI:
- 10.1063/1.1544084

[22]

Electrical and mechanical properties of C70 fullerene and graphite under high pressures studied using designer diamond anvils

J.R. Patterson
,
S.A. Catledge
,
Y.K. Vohra
,
J. Akella
,
S.T. Weir

- Phys.Rev.Lett. 85 (2000) 5364-5367
•
DOI:
- 10.1103/PhysRevLett.85.5364

[23]

Epitaxial diamond encapsulation of metal microprobes for high pressure experiments

S.T. Weir
,
J. Akella
,
C. Aracne-Ruddle
,
Y.K. Vohra
,
S.A. Catledge

- Appl.Phys.Lett. 77 (2000) 3400
•
DOI:
- 10.1063/1.1326838

[24]

Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions

H.K. Mao
,
J. Xu
,
P.M. Bell

•
DOI:
- 10.1029/JB091iB05p04673

[25]

Solidification of high-pressure medium Daphne 7373

K. Yokogawa
,
K. Murata
,
H. Yoshino
,
S. Aoyama

•
DOI:
- 10.1143/JJAP.46.3636

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